HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1-methylpyridin-2(1H)-one → HCID 68759408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1-methylpyridin-2(1H)-one | HCID 22132396 | — |
| Reactant | HCID 68758548 | HCID 68758548 | — |
| Product | HCID 68759408 | HCID 68759408 | — |
Reaction Steps
The title compound was prepared from 3-{cyclopropyl-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]methyl}-6-(2-hydroxy-2-methyl-propyl)-6-phenyl-[1,3]oxazinan-2-one (for preparation see below) and 4-bromo-1-methyl-1H-pyridin-2-one following a procedure analogous to that described in Example 3. LC-MS (Method 1): tR=3.57 min; Mass spectrum (ESI+): m/z=487 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703765B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-2d65dd8502d44cdcba8ad0150ad10aba |
| Source note | uspto-grants-2014_04 |