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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2368048Generated: October 30, 2026

4-Bromo-1-methylpyridin-2(1H)-one → HCID 68759408, compound

https://huagongshe.com/reaction/2368048

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Bromo-1-methylpyridin-2(1H)-oneHCID 22132396—
ReactantHCID 68758548HCID 68758548—
ProductHCID 68759408HCID 68759408—

Reaction Steps

The title compound was prepared from 3-{cyclopropyl-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]methyl}-6-(2-hydroxy-2-methyl-propyl)-6-phenyl-[1,3]oxazinan-2-one (for preparation see below) and 4-bromo-1-methyl-1H-pyridin-2-one following a procedure analogous to that described in Example 3. LC-MS (Method 1): tR=3.57 min; Mass spectrum (ESI+): m/z=487 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08703765B2
Source datasetuspto-grants-2014_04
ORD IDord-2d65dd8502d44cdcba8ad0150ad10aba
Source noteuspto-grants-2014_04