Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2368049Generated: October 29, 2026

5-Bromo-1-methylpyridin-2(1H)-one → HCID 68759699, compound

https://huagongshe.com/reaction/2368049

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Bromo-1-methylpyridin-2(1H)-oneHCID 13024027—
ReactantHCID 68759408HCID 68759408—
ProductHCID 68759699HCID 68759699—

Reaction Steps

The title compound was prepared from 3-{cyclopropyl-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]methyl}-6-(2-hydroxy-2-methyl-propyl)-6-phenyl-[1,3]oxazinan-2-one (for preparation see Example 3) and 5-bromo-1-methyl-1H-pyridin-2-one following a procedure analogous to that described in Example 3. LC-MS (Method 1): tR=3.34 min; Mass spectrum (ESI+): m/z=487 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08703765B2
Source datasetuspto-grants-2014_04
ORD IDord-85fc93f6c97340e482513021c86279b9
Source noteuspto-grants-2014_04