HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-1-methylpyridin-2(1H)-one → HCID 68759699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-1-methylpyridin-2(1H)-one | HCID 13024027 | — |
| Reactant | HCID 68759408 | HCID 68759408 | — |
| Product | HCID 68759699 | HCID 68759699 | — |
Reaction Steps
The title compound was prepared from 3-{cyclopropyl-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]methyl}-6-(2-hydroxy-2-methyl-propyl)-6-phenyl-[1,3]oxazinan-2-one (for preparation see Example 3) and 5-bromo-1-methyl-1H-pyridin-2-one following a procedure analogous to that described in Example 3. LC-MS (Method 1): tR=3.34 min; Mass spectrum (ESI+): m/z=487 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703765B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-85fc93f6c97340e482513021c86279b9 |
| Source note | uspto-grants-2014_04 |