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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 236812Generated: October 31, 2026

Sulfuryl chloride → HCID 12581868, compound

https://huagongshe.com/reaction/236812

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfuryl chlorideHCID 24648—
ReactantHCID 12581860HCID 12581860—
SolventDichloromethaneHCID 6344—
ProductHCID 12581868HCID 12581868—

Reaction Steps

An 8.0 g. portion of thieno[3,4-b][1,5]benzoxazepin-10(9H)-one is suspended in 364 ml. of methylene chloride. A 3.27 ml. portion of sulfuryl chloride is added dropwise and the mixture is stirred overnight. The solid is collected and washed with methylene chloride, giving 3-chloro-thieno[3,4-b][1,5]benzoxazepin-10(9H)-one.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04157444
Source datasetuspto-grants-1979_06
ORD IDord-01e344525ecb49d88c449d4a323f91d4
Source noteuspto-grants-1979_06