HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 21315985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 12703384 | HCID 12703384 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21315985 | HCID 21315985 | — |
Reaction Steps
A 4.0 g. portion of 7-chloro-thieno[3,4-b][1,5]benzoxazepin-10(9H)-one (Example 4) and 4.0 g. of phosphorus pentachloride in 100 ml. of dry toluene are refluxed for 41/2 hours concentrated and triturated with toluene, giving 7,10-dichlorothieno[3,4-b][1,5]benzoxazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04157444 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-4ee08cdfdf7a4a91afac86b13b1c24d1 |
| Source note | uspto-grants-1979_06 |