HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178467816, compound → HCID 178467817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178467816 | HCID 178467816 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178467817 | HCID 178467817 | 95.9% |
Reaction Steps
A mixture of (3E)-4-{trans-4-[6-(cyclopropylmethoxy)-2H-indazol-2-yl]cyclohexyl}but-3-en-2-one (2.85 g), palladium-activated carbon ethylenediamine complex (0.538 g) and ethyl acetate (100 mL) was stirred at room temperature for 15 hr under a hydrogen atmosphere. The catalyst was removed by filtration, and the filtrate was concentrated under reduced pressure to give the title compound (2.75 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703758B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-11604b866a2a4570b9f441c14b09ff5e |
| Source note | uspto-grants-2014_04 |