HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 12581869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 12581867 | HCID 12581867 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 12581869 | HCID 12581869 | — |
Reaction Steps
A suspension of 1.16 g. of thieno[3,4-b][1,5]-benzothiazepin-10(9H)-one in 20 ml. of methylene chloride was treated with 0.81 g of sulfuryl chloride as in Example 12 to give 3-chlorothieno[3,4-b][1,5]benzothiazepin-10(9H)-one as a white crystal, m.p. 287°-288° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04157444 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-69d7eb3b457e456184bd55ec9f0e45f3 |
| Source note | uspto-grants-1979_06 |