Thionyl Chloride → HCID 86664890, compound

HRID 2368655Notes

Reaction equation

HRID 2368655 reaction equation
[NH2:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6](O)=[O:7])=[CH:4][N:3]=1.S(Cl)([Cl:16])=O>>[NH2:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6]([Cl:16])=[O:7])=[CH:4][N:3]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 2718816-Amino-5-nitronicotinic acid

Product 1

HCID 86664890HCID 86664890, compound

Procedure

6-amino-5-nitro-nicotinic acid (2.50 g, 13.7 mmol) was mixed with 50 mL thionyl chloride and refluxed for 2 h. The mixture was concentrated and the residue reacted without further purification.

Workup

  1. temperaturerefluxed for 2 h
  2. concentrationThe mixture was concentrated
  3. customthe residue reacted without further purification

Sources & evidence

ORD record
ord-dd601a37e06846f2a3aa380579675d65
Source dataset
uspto-grants-2014_04
Patent number
US08703796B2

Reaction notes

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