HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86664890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-Amino-5-nitronicotinic acid | HCID 271881 | — |
| Product | HCID 86664890 | HCID 86664890 | — |
Reaction Steps
6-amino-5-nitro-nicotinic acid (2.50 g, 13.7 mmol) was mixed with 50 mL thionyl chloride and refluxed for 2 h. The mixture was concentrated and the residue reacted without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703796B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-dd601a37e06846f2a3aa380579675d65 |
| Source note | uspto-grants-2014_04 |