HCID 67355593, compound → HCID 67356619, compound

HRID 2368665Notes

Reaction equation

HRID 2368665 reaction equation
[NH2:1][C:2]1[C:11]([N+:12]([O-])=O)=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[C:4]([O:15][CH2:16][CH2:17][O:18][CH3:19])[N:3]=1>[Pd].C1COCC1.CO>[NH2:12][C:11]1[C:2]([NH2:1])=[N:3][C:4]([O:15][CH2:16][CH2:17][O:18][CH3:19])=[C:5]([CH:10]=1)[C:6]([O:8][CH3:9])=[O:7]

Participants

5

Reactant 1

HCID 67355593HCID 67355593, compound

Product 1

HCID 67356619HCID 67356619, compound

Reagents, catalysts & solvents 3

HCID 23938PalladiumCatalystHCID 887MethanolSolventHCID 8028TetrahydrofuranSolvent

Procedure

Prepared analogously to example 154d by hydrogenation of the product obtained in (800d) using palladium on charcoal in THF and methanol.

Workup

  1. customPrepared analogously to example 154d by hydrogenation of the product

Sources & evidence

ORD record
ord-f30c214937684c8fb8b959dfba673998
Source dataset
uspto-grants-2014_04
Patent number
US08703796B2

Reaction notes

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