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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 236878Generated: October 31, 2026

Hydrochloric Acid → HCID 21315534, compound

https://huagongshe.com/reaction/236878

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant4-CyanopyridineHCID 7506—
Reactant2-VinylpyridineHCID 7521—
SolventIsopropanolHCID 3776—
ProductHCID 21315534HCID 21315534—

Reaction Conditions

Temperature25 °C

Reaction Steps

To 166.4 parts of 4-cyanopyridine in 500 cc of isopropanol was added 170 parts of a 15.9% solution of hydrogen chloride in isopropanol. To this was added 292 parts of 2-vinylpyridine in 500 cc of isopropanol, and the resulting mixture heated to reflux for 5.5 hours. The reaction was cooled to 25° C. and 261 parts of 1-[2-(2-pyridyl)ethyl]-4-cyanopyridinium chloride hydrochloride isolated on filtration.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04158093
Source datasetuspto-grants-1979_06
ORD IDord-d2e3df6f18d2475482f8a82788e707fb
Source noteuspto-grants-1979_06