HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68227296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68227587 | HCID 68227587 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68227296 | HCID 68227296 | — |
Reaction Steps
The title compound was prepared in analogy to example 1, step 5 from 10-{4-[(R)-2,2,2-trifluoro-1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-1,4-dioxa-10-aza-dispiro[4.2.4.2]tetradecan-9-one (4.91 g) by treatment with 2 M HCl (58.3 ml) in THF (68.2 ml) as a white solid. (3.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703807B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-b74cc24a2c14424bb5732972b261db97 |
| Source note | uspto-grants-2014_04 |