HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 59632481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 59632103 | HCID 59632103 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 59632481 | HCID 59632481 | — |
Reaction Steps
A solution of 5-(4-bromophenyl)-1-(2-chloroethyl)-3-(trifluoromethyl)-1H-pyrazole (200 mg, 0.56 mmol) and morpholine (0.245 mL, 5 equiv) in acetonitrile (2 mL) was stirred overnight at 90° C. Evaporation of solvent gave of 4-(2-(5-(4-bromophenyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl)ethyl)morpholine. MS (ES): 404 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703805B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-751d16c7179c45e2b46810f87a39aed1 |
| Source note | uspto-grants-2014_04 |