Hydrochloric Acid → HCID 12126688, compound

HRID 236927Notes

Reaction equation

HRID 236927 reaction equation
[C:1]1([NH:15][C:16](=[O:22])[C:17]([O:19]CC)=[O:18])[CH:6]=[CH:5][CH:4]=[C:3]([NH:7][C:8](=[O:14])[C:9]([O:11]CC)=[O:10])[CH:2]=1.Cl>[OH-].[Na+].O>[C:1]1([NH:15][C:16](=[O:22])[C:17]([OH:19])=[O:18])[CH:6]=[CH:5][CH:4]=[C:3]([NH:7][C:8](=[O:14])[C:9]([OH:11])=[O:10])[CH:2]=1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 12897298HCID 12897298, compound

Product 1

HCID 12126688HCID 12126688, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 14798Sodium HydroxideSolvent

Procedure

Diethyl N,N'-(m-phenylene)dioxamate (1.0 gram) is stirred in 1.0N aqueous sodium hydroxide for 0.5 hour. The solution is diluted with water (100 ml.) and the pH adjusted to pH 3 with concentrated hydrochloric acid. The resulting precipitate is collected and recrystallized from ethanol (0.46 grams, M. P. 240° C.).

Workup

  1. customThe resulting precipitate is collected
  2. customrecrystallized from ethanol (0.46 grams, M. P. 240° C.)

Sources & evidence

ORD record
ord-29743003795943118e146580f5e51081
Source dataset
uspto-grants-1979_06
Patent number
US04159278

Reaction notes

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