HRID236948

反应详情

EQUATION

反应方程式

HRID 236948 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of the product of step (e) (0.3 g), in water (25 ml) was acidified with 2 N hydrochloric acid. The precipitated organic acid was filtered off washed with water and dried to give the title compound as a white solid, (0.24 g), mp 245°-8°.

WORKUP

后处理

  1. filtrationThe precipitated organic acid was filtered off
  2. washwashed with water
  3. customdried