HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 20304561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 20304522 | HCID 20304522 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20304561 | HCID 20304561 | 84.1% |
Reaction Steps
A mixture of the product of step (b) (3.0 g) and sodium bicarbonate (3.0 g) in water (100 ml) was heated at reflux for 3 hours. The solution was cooled and acidified and the resulting white solid was filtered and dried to give the title compound 2.4 g (84%), mp 269°-271°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159273 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-a2ec43410cb94413a17eb3f9e7321254 |
| Source note | uspto-grants-1979_06 |