HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 21314613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20304527 | HCID 20304527 | — |
| Product | HCID 21314613 | HCID 21314613 | 72.3% |
Reaction Steps
The product of step (a) (5.3 g) was treated with sodium (2.3 g) and diethyl oxalate (7.3 g) under the conditions of Example 1(d) to give the title ester (5.0 g; 72%), mp 130°-132°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159273 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-5a5a52306df64f45b3f468e9e863d39b |
| Source note | uspto-grants-1979_06 |