Sodium Bicarbonate → HCID 23716997, compound

HRID 236962Notes

Reaction equation

HRID 236962 reaction equation
C(=O)(O)[O-].[Na+:5].[CH3:6][C:7]1[C:8](=[O:27])[C:9]2[CH:23]=[C:22]3[C:17]([CH2:18][CH2:19][CH2:20][CH2:21]3)=[C:16]([CH2:24][CH2:25][CH3:26])[C:10]=2[O:11][C:12]=1[C:13]([OH:15])=[O:14]>O>[CH3:6][C:7]1[C:8](=[O:27])[C:9]2[CH:23]=[C:22]3[C:17]([CH2:18][CH2:19][CH2:20][CH2:21]3)=[C:16]([CH2:24][CH2:25][CH3:26])[C:10]=2[O:11][C:12]=1[C:13]([O-:15])=[O:14].[Na+:5]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 20304505HCID 20304505, compound

Product 1

HCID 23716997HCID 23716997, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of sodium bicarbonate (0.78 g) in water (30 ml) was added to the product of step (g) (2.8 g). The resulting solution was filtered then evaporated to small volume and diluted with acetone. Crystallisation occurred and the resulting crystals were filtered off and recovered as an off-white solid, which was the desired sodium salt (2.65 g).

Workup

  1. filtrationThe resulting solution was filtered
  2. customthen evaporated to small volume
  3. additiondiluted with acetone
  4. customCrystallisation
  5. filtrationthe resulting crystals were filtered off
  6. customrecovered as an off-white solid, which

Sources & evidence

ORD record
ord-105ae161a11e4b6f801ee3bdf9499cea
Source dataset
uspto-grants-1979_06
Patent number
US04159273

Reaction notes

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