Sodium Bicarbonate → HCID 23717000, compound
Reaction equation
[Cl:1][CH2:2][CH:3]([OH:23])[CH2:4][C:5]1[C:14]2[O:15][C:16]([C:20]([OH:22])=[O:21])=[CH:17][C:18](=[O:19])[C:13]=2[CH:12]=[C:11]2[C:6]=1[CH2:7][CH2:8][CH2:9][CH2:10]2.C(=O)(O)[O-].[Na+:28]>O>[Cl:1][CH2:2][CH:3]([OH:23])[CH2:4][C:5]1[C:14]2[O:15][C:16]([C:20]([O-:22])=[O:21])=[CH:17][C:18](=[O:19])[C:13]=2[CH:12]=[C:11]2[C:6]=1[CH2:7][CH2:8][CH2:9][CH2:10]2.[Na+:28]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
To a suspension of the acid from step (a) (1.474 g) in water (30 ml) was added sodium bicarbonate (0.368 g) and the resulting solution was freeze-dried. The solid obtained was dried in vacuo to give the required salt, 1.4 g (89%).
Workup
- customthe resulting solution was freeze-dried
- customThe solid obtained
- customwas dried in vacuo
Sources & evidence
- ORD record
- ord-032d89bdb59f42cf9e592ac35c4b9c88
- Source dataset
- uspto-grants-1979_06
- Patent number
- US04159273
Reaction notes
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