HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178445811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 4-tert-Butylcyclohexanol | HCID 7391 | — |
| Reactant | Succinic anhydride | HCID 7922 | — |
| Product | HCID 178445811 | HCID 178445811 | — |
Reaction Steps
1 g 4-tert.-Butyl-cyclohexanol (cis/trans 30:70; i.e. 1 eq) was mixed with 10 ml toluene (i.e. 0.6 mol). 0.5 g succinic anhydride (i.e. 0.8 eq) and 0.1 g lipase immobilized on Na2SO4 were added (i.e. 10% per weight). The reaction conditions were the same as in example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08709751B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-0b05620fa57843f68d8882b066dbdb2f |
| Source note | uspto-grants-2014_04 |