HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86647139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86647138 | HCID 86647138 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86647139 | HCID 86647139 | — |
Reaction Steps
3-(Boc-aminoethyl-methyl-amino)-propionic acid tert-butyl ester (630 mg, 2.1 mmol) was treated with trifluoroacetic acid (6 mL) for 2 hours. 3-(Aminoethyl-methyl-amino)-propionic acid trifluoroacetic acid salt was isolated by recrystallisation from THF to give a white powder, 974 mg (quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08710000B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-859adf4764d840e8856dd7d735fa35cc |
| Source note | uspto-grants-2014_04 |