HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 20290839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 12751641 | HCID 12751641 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20290839 | HCID 20290839 | — |
Reaction Steps
To a solution of 70.0 g (0.32 mole) of 2-(4-fluorophenyl-1-(2-thienyl)ethanone in 600 ml of ether was added dropwise a solution of 56.0 g (0.35 mole) of bromine in 120 ml of methylene chloride at room temperature. The reaction mixture was concentrated under vacuum to give 123.0 g of 2-bromo-2-(4-fluorophenyl)-1-(2-thienyl)ethanone as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159338 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-40333d8475ee4c45a9b7aee47164a2ad |
| Source note | uspto-grants-1979_06 |