HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium thiocyanate → HCID 178505564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium thiocyanate | HCID 15666 | — |
| Reactant | HCID 21314975 | HCID 21314975 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | HCID 178505564 | HCID 178505564 | — |
Reaction Steps
Alternatively, reaction of 63.4 g (0.27 mole) of 2-(4-fluorophenyl)-2-hydroxy-1-(2-thienyl)ethanone with 29.0 g (0.38 mole) of ammonium thiocyanate in 1-propanol gave 71.6 g of 4-(4-fluorophenyl)-5-(2-thienyl)-1H-2-imidazolethiol, m.p. 275°-277° (Recrystallized from 1-butanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159338 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-65b63310b8494152a608b7fa6b70d224 |
| Source note | uspto-grants-1979_06 |