HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 72673270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 70662762 | HCID 70662762 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 72673270 | HCID 72673270 | — |
Reaction Steps
Compound 1 was co-precipitated with equal mole of methane sulfonic acid in DMF to get yellow powder as salt product Compound 2. mp 278° C.; 1H-NMR (400 MHz, DMSO): δ 2.31 (s, 3H), 5.52 (s, 2H), 6.73 (s, 1H), 6.80 (s, 1H), 7.30-8.80 (m, 12H), 10.28 (s, 1H), 12.29 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08710062B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-62170ecf684c4617be0d737d5dc67c51 |
| Source note | uspto-grants-2014_04 |