Hydrochloric Acid → HCID 67450266, compound

Participants

Reaction Steps

Add HCl (2.0 M solution in ether) (0.018 g, 0.0005 mol, 1.0 eq) to a solution of 8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)-9-(2-(methylsulfonyl)ethyl)-9H-purine (0.24 g, 0.0005 mol) in ether (4 mL) at 0° C. and stir for 2 h at room temperature. Filter the precipitate and wash with ether and dry under vacuum to provide the title compound (0.15 g) as white solid. ES/MS m/z 449 (M+1).

Provenance & Evidence