Hydrochloric Acid → HCID 67446835, compound

Participants

Reaction Steps

Add HCl (2.0 M solution in ether) (0.027 g, 0.7 mmol) to a mixture of 2-[8-(2-chlorophenyl)-6-(4-ethylpiperazin-1-yl)-2-methyl-purin-9-yl]ethanamine (0.3 g, 0.7 mmol) in ether (5 mL) at 0° C. and stir for 2 h at room temperature. Collect the precipitate by filtration and wash with ether. Dry under vacuum to give the title compound (0.25 g) as a white solid. ES/MS m/z 400 (M+1).

Provenance & Evidence