Hydrochloric Acid → HCID 67449589, compound

Participants

Reaction Steps

Add HCl (2.0 M solution in ether) (0.024 g, 0.0006 mol) to a solution of methyl N-[2-[8-(2-chlorophenyl)-2-methyl-6-(4-methylpiperazin-1-yl)purin-9-yl]ethyl]carbamate (0.3 g, 0.0006 mol) in ether (6 mL) at 0° C. and stir for 2 h at room temperature. Filter the precipitate, wash with ether, and dry under vacuum to afford the title compound (0.28 g) as a white solid. ES/MS m/z 444 (M+1).

Provenance & Evidence