HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoroethylene → HCID 178506050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoroethylene | HCID 8301 | — |
| Reactant | HCID 178527827 | HCID 178527827 | — |
| Product | HCID 178506050 | HCID 178506050 | — |
Reaction Steps
4-Phenyl-5-(3-pyridyl)-1H-2-imidazolethiol (2.0 g; 7.9 mmoles) was reacted with 5.0 g (50 mmoles) of tetrafluoroethylene and the crude product purified by chromatography on Silicar CCNo. 7 with chloroform to afford 800 mg of 4-phenyl 5-(3-pyridyl)-2-(1,1,2,2-tetrafluoroethylthio)-1H-imidazole, m.p. 153°-154° (recrystallized from toluene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159338 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-8b2fab2b9f544b839f052518bb73d201 |
| Source note | uspto-grants-1979_06 |