Lawesson's reagent → HCID 88868299, compound

Participants

Reaction Steps

A solution of Example 1D (0.730 g, 2.123 mmol) and Lawesson's reagent (0.515 g, 1.274 mmol) in toluene (40 mL) was heated to reflux for 4 hours. The reaction mixture was concentrated and purified on a 40 g column using the ISCO Companion flash system eluting with hexane/ethyl acetate (1:1 to 4:6) to provide the title compound.

Provenance & Evidence