Hydrochloric Acid → HCID 178511689, compound

Participants

Reaction Steps

18 mg (0.05 mmol) trans-[4-(5-Chloro-isoquinolin-6-yloxy)-cyclohexyl]-carbamic acid tert-butyl ester (10) were stirred in 2 M HCl at room temperature. After 2 days, the solvent was removed i. vac. and the residue was purified by preparative HPLC. 8 mg of the title compound could be obtained as trifluoro acetate. Rt=0.69 min (Method #1). Detected mass: 277.2/279.2 (M+H+).

Provenance & Evidence