HRID237091
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
A mixture of 0.57 g. of 5-(p-fluorophenyl)-3-hydrazino-1,2,4-triazine and 20 ml. of ethyl orthoacetate is refluxed for 4 hours, cooled and filtered. The desired product is recovered as a brown solid, m.p. 227.5°-231° C.
WORKUP
后处理
- additionA mixture of 0.57 g
- temperaturecooled
- filtrationfiltered
- customThe desired product is recovered as a brown solid, m.p. 227.5°-231° C.