Hydrazine hydrate (1:1) → HCID 12581289, compound

HRID 237101Notes

Reaction equation

HRID 237101 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=2[Cl:14])=[CH:6][N:7]=1.O.[NH2:16][NH2:17]>N1C=CC=CC=1>[Cl:14][C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=1[C:5]1[N:4]=[N:3][C:2]([NH:16][NH2:17])=[N:7][CH:6]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 125812883-Chloro-6-(o-chlorophenyl)-1,2,4-triazine

Product 1

HCID 12581289HCID 12581289, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A solution of 19.8 g. of 3-chloro-6-(o-chlorophenyl)-1,2,4-triazine in 120 ml. of pyridine is treated with 15 g. of hydrazine hydrate as described in Example 12, giving 6-(o-chlorophenyl)-3-hydrazino-1,2,4-triazine as yellow needles.

Sources & evidence

ORD record
ord-f89f9d0324f540ee9bbb1d6489d22c95
Source dataset
uspto-grants-1979_06
Patent number
US04159375

Reaction notes

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