Ammonium Acetate → HCID 13121517, compound

HRID 237125Notes

Reaction equation

HRID 237125 reaction equation
[O:1]=[C:2]1O[C:6]([C:8]([O:10][CH2:11][CH3:12])=[O:9])=[N:5][C:4]2[S:13][C:14]([CH2:16][CH2:17][CH3:18])=[CH:15][C:3]1=2.C([O-])(=O)C.[NH4+:23]>C(O)(=O)C>[O:1]=[C:2]1[NH:23][C:6]([C:8]([O:10][CH2:11][CH3:12])=[O:9])=[N:5][C:4]2[S:13][C:14]([CH2:16][CH2:17][CH3:18])=[CH:15][C:3]1=2

Participants

4

Reactant 2

HCID 517165Ammonium AcetateHCID 13121569HCID 13121569, compound

Product 1

HCID 13121517HCID 13121517, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The product of Procedure 85 is converted to the desired product by treatment with ethanolic ammonium acetate according to the method of Procedure 5 except that acetic acid is omitted. The product is recrystallized from ethanol, m.p. 169°-170° C.

Sources & evidence

ORD record
ord-c62716f1af964d5b948da1e3124615b3
Source dataset
uspto-grants-1979_06
Patent number
US04159377

Reaction notes

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