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HRID2371306

反应详情

EQUATION

反应方程式

HRID 2371306 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：C=CCOc1ccc(C[C@H](NC(=O)OC(C)(C)C)C(=O)N[C@@H](CC(C)C)C(=O)OC)cc1
HCID86650238

未命名化合物

PRODUCTS

生成物

1
结构：C=CCOc1ccc(C[C@H](N)C(=O)N[C@@H](CC(C)C)C(=O)OC)cc1.Cl
HCID66847093

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

Methyl ester 1 (4.00 g, 8.92 mmol) was dissolved in 4M HCl in 1,4-dioxane (20 mL). The resultant solution was stirred at rt for 18 h before being concentrated in vacuo to yield a white solid, 3.43 g, 100%.

WORKUP

后处理

  1. concentrationbefore being concentrated in vacuo
  2. customto yield a white solid, 3.43 g, 100%