Acetone → HCID 86736124, compound

HRID 237138Notes

Reaction equation

HRID 237138 reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[OH-].[Li+:9].C[C:11](C)=[O:12]>CO>[C:4]([O:12][CH3:11])(=[O:5])/[CH:3]=[CH:2]\[C:1]([O-:6])=[O:7].[Li+:9]

Participants

5

Reactant 3

HCID 180AcetoneHCID 3939Lithium Hydroxide2×HCID 7923Maleic Anhydride

Product 1

HCID 86736124HCID 86736124, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Twenty grams of maleic anhydride is dissolved in 200 mls methanol, 4.8 grams (0.2 moles) lithium hydroxide is added. The mixture is stirred until all the lithium hydroxide dissolves (at this point the pH reads 7.0). To the solution is added acetone and the solid is filtered and dried. 23 grams product is obtained.

Workup

  1. dissolutiondissolves (at this point the pH
  2. filtrationthe solid is filtered
  3. customdried

Sources & evidence

ORD record
ord-7012308247924baeaa9649bf8ebc0d9d
Source dataset
uspto-grants-1979_06
Patent number
US04159388

Reaction notes

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