HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 556978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-((5-Methyl-2-(1-methylethyl)cyclohexyl)oxy)acetic acid | HCID 97814 | — |
| Product | HCID 556978 | HCID 556978 | 107.4% |
Reaction Steps
0.771 g (3.6 mmol) of (-)-menthoxyacetic acid is stirred under reflux with 2.1 g of thionyl chloride for 4 to 5 h. The thionyl chloride is first removed from the solution by distillation under reduced pressure. 3 ml of dry benzene are then added in order to remove residual thionyl chloride by means of vacuum distillation. 0.9 g of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05093350 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-e451021af54e4d49b89adeba7e1e916b |
| Source note | uspto-grants-1992_03 |