Pyridine → HCID 67903428, compound

Participants

Reaction Steps

First, 320 mg of 1,4-bis(3-bromopropyl)benzene was dissolved in 5.0 ml of ethanol, 202 μl of pyridine was added thereto, the mixture was then refluxed for 18 hours. After cooling, to the reaction mixture was added 20 ml of ethyl ether. The resulting solids were recrystallized from ethanol/ethyl ether to obtain 215 mg of the title compound as a colorless crystal.

Provenance & Evidence