1-Methyl-1,2-dihydropyridine → HCID 86745532, compound

Participants

Reaction Steps

To a solution of 376 mg of 1,4-bis(5-bromopentyl)benzene in 2 ml of absolute ethanol, 365 μl of N-methylpyridine was added, and the mixture was refluxed for 5 hours. After concentration under a reduced pressure and addition of acetone, and the mixture was allowed to stand overnight. The product was filtered and recrystallized from ethanol (0.5 ml)--acetone (2 ml) to obtain 455 mg of the title compound as a colorless crystal.

Provenance & Evidence