Methyl iodide → HCID 19907342, compound

Participants

Reaction Steps

To a solution of 193 mg of N,N-dimethyl-8-phenyloctylamine in 1.5 ml of absolute methanol, were added dropwise 258 μl of methyl iodide, and the mixture was stirred at a room temperature for 6.5 hours. After adding 3 ml of ethyl acetate, the mixture was stirred with ice-cooling for 30 minutes. Resulting crystal was filtered, washed with ethyl acetate, and dried under a reduced pressure to obtain 238 mg of the title compound as a colorless crystal.

Provenance & Evidence