Ethanol → HCID 67903179, compound

Participants

Reaction Steps

First, 0.56 g of 1,4-bis(diethylaminobutyl)benzene and 2.1 g of ethyl iodide were dissolved in 7 ml of absolute ethanol, and the mixture was refluxed for 4 hours. After removing the solvent under a reduced pressure and adding acetone and a small amount of ethanol, the mixture was stirred at a room temperature for 30 minutes. The resulting crystal was filtered, washed with acetone, and dried under a reduced pressure to obtain 0.335 g of the title compound as a pale yellow crystal.

Provenance & Evidence