N-Methylpiperidine → HCID 19907488, compound

Participants

Reaction Steps

First, 0.35 g of 1,4-bis(4-bromobutyl)benzene and 0.5 g of N-methylpiperidine were dissolved in 5 ml of absolute ethanol, the solution was refluxed for 9 hours, and evaporated under a reduced pressure. To the residue were added acetone and a small amount of ethanol, and the mixture was stirred at a room temperature for 30 minutes. The resulting crystal was filtered, washed with acetone and dried under a reduced pressure to obtain 0.47 g of the title compound as a colorless crystal.

Provenance & Evidence