HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19907475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 19907397 | HCID 19907397 | — |
| Product | HCID 19907475 | HCID 19907475 | — |
Reaction Steps
To solution of 97 mg of 1,4-bis(7-diethylaminoheptyl)benzene in 1 ml of absolute ethanol, was added 187 μl of ethyl iodide, and the mixture was refluxed for 3 hours and evaporated under a reduced pressure. After adding acetone, the mixture was concentrated and allowed to stand in a freezer for a week to obtain 152 mg of the title compound as a pale brown crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05093370 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-8ea9848004e54a2a998631496a021e58 |
| Source note | uspto-grants-1992_03 |