HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 19907368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 19907346 | HCID 19907346 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19907368 | HCID 19907368 | — |
Reaction Steps
To a solution of 78 mg of 2,6-bis(3-diethylaminopropyl)naphthalene in 1 ml of absolute ethanol was added 176 μl of ethyl iodide, and the mixture was refluxed for 140 minutes and cooled. After adding 2 ml of acetone, the mixture was stirred for 20 minutes. The resulting crystal was collected by filtration, washed with acetone and dried under a reduced pressure to obtain 117 mg of the title compound as a colorless crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05093370 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-55c17812c60740b4bfc2feab140dd78e |
| Source note | uspto-grants-1992_03 |