4-Bromophenol → 1-Bromo-4-(3-bromopropoxy)benzene

HRID 2371614Notes

Reaction equation

HRID 2371614 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][CH:3]=1>C(Cl)Cl.CCCCCC>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:4][CH2:3][CH2:2][Br:1])=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 78084-Bromophenol

Product 1

HCID 3479241-Bromo-4-(3-bromopropoxy)benzene

Reagents, catalysts & solvents 1

HCID 21226440Methylenechloride HexaneSolvent

Procedure

The title compound was prepared and worked up by the method of Example 6 using 4-bromophenol in place of 3,4-dichlorophenol. After chromatography the title compound (3.45 g) was found to be homogeneous by thin layer chromatography (10% by volume of methylene chloride/hexane on silica gel plates).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-e93cef3734e14bd685436327d51f1575
Source dataset
uspto-grants-1992_03
Patent number
US05093353

Reaction notes

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