HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 19985186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzoic acid, 2-(dodecyloxy)- | HCID 289454 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19985186 | HCID 19985186 | — |
Reaction Steps
29.1 g of the dodecyloxybenzoic acid was dissolved in 300 ml of methylene chloride, 1 ml of N,N-dimethylformamide was added, and 24 g of thionyl chloride was added dropwise over about 30 min under heating and reflux. After the addition the heating and refluxing were continued for 2 hours further, and concentration was conducted, to obtain 2-dodecyloxybenzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05094938 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-5478a2c45fc74b69a27fcc1927b2ff54 |
| Source note | uspto-grants-1992_03 |