HRID237190
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 75 °C
PROCEDURE
实验过程
Next, 130.5 g of poly(p-tert-butoxystyrene/cyclohexyl acrylate) was suspended in isopropanol. Subsequently, 30 ml of concentrated hydrochloric acid was added to the suspension, and agitated at 70 to 80° C. for four hours. The reaction liquid was cooled, and poured in 1500 ml of water, thereby precipitating a reaction product. The precipitated solid was collected by filtration, washed with water, and dried in vacuum. Thus, 85.5 g of poly(p-hydroxystyrene/cyclohexyl acrylate) was obtained as a white powdery crystal.
WORKUP
后处理
- customThe reaction liquid
- temperaturewas cooled
- customprecipitating a reaction product
- filtrationThe precipitated solid was collected by filtration
- washwashed with water
- customdried in vacuum