HRID237190

反应详情

EQUATION

反应方程式

HRID 237190 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

CONDITIONS

反应条件

温度
75 °C

PROCEDURE

实验过程

Next, 130.5 g of poly(p-tert-butoxystyrene/cyclohexyl acrylate) was suspended in isopropanol. Subsequently, 30 ml of concentrated hydrochloric acid was added to the suspension, and agitated at 70 to 80° C. for four hours. The reaction liquid was cooled, and poured in 1500 ml of water, thereby precipitating a reaction product. The precipitated solid was collected by filtration, washed with water, and dried in vacuum. Thus, 85.5 g of poly(p-hydroxystyrene/cyclohexyl acrylate) was obtained as a white powdery crystal.

WORKUP

后处理

  1. customThe reaction liquid
  2. temperaturewas cooled
  3. customprecipitating a reaction product
  4. filtrationThe precipitated solid was collected by filtration
  5. washwashed with water
  6. customdried in vacuum