HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 131717192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Tris(hydroxymethyl)aminomethane | HCID 6503 | — |
| Reactant | 131817-86-2 | HCID 6439321 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131717192 | HCID 131717192 | — |
Reaction Steps
(E)-3-[4-(2,5-dimethyl-1H-pyrrol-1-yl)phenyl]-N-methyl-2-propenohydroxamic acid (1.85 g) is added to a solution of 0.85 g of tromethamine in 150 ml of methanol. The resulting solution is treated with charcoal, filtered and evaporated to dryness. The residue is crystallized from ether to obtain (E)-3-[4-(2,5-dimethyl-1H-pyrrol-1-yl)phenyl]-N-methyl-2-propenohydroxamic acid tromethamine salt, m.p. 134°-136°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05096919 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-c40514f2e6f6453a99fcc6a2dca970c0 |
| Source note | uspto-grants-1992_03 |