HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2371983Generated: October 29, 2026
3-Methylbenzoyl chloride → HCID 14366279, compound
https://huagongshe.com/reaction/2371983
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Methylbenzoyl chloride | HCID 74375 | — |
| Reactant | 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin | HCID 11436148 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14366279 | HCID 14366279 | — |
Reaction Steps
46.6 g (0.3 mol) of 3-methylbenzoyl chloride were warmed to 85° C. under a nitrogen atmosphere. 69 g (0.3 mol) of 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin were added dropwise while stirring. The temperature was then increased in steps to 115° C. When the reaction was complete, 50 ml of toluene were added at room temperature. After crystallization, 85 g (84% of theory) of the abovementioned compound of melting point 108° to 111° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05096935 |
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| Source dataset | uspto-grants-1992_03 |
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| ORD ID | ord-31a77cc2be784d448c2fe850b5debb09 |
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| Source note | uspto-grants-1992_03 |
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