HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2371987Generated: October 31, 2026
3,5-Dimethylbenzoyl Chloride → HCID 14366285, compound
https://huagongshe.com/reaction/2371987
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3,5-Dimethylbenzoyl Chloride | HCID 81088 | — |
| Reactant | 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin | HCID 11436148 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14366285 | HCID 14366285 | — |
Reaction Steps
67.4 g (0.4 mol) of 3,5-dimethylbenzoyl chloride were warmed to 80° C. under a nitrogen atmosphere. 92 g (0.4 mol) of 6-methoxy-(6H)-dibenz[c,e][1,2]oxaphosphorin were added dropwise while stirring. The temperature during the addition was increased in steps to 115° C. When the reaction was complete, 50 ml of acetone were added at room temperature. After crystallization, 113 g (81% of theory) of the abovementioned compound of melting point 120° to 124° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05096935 |
|---|
| Source dataset | uspto-grants-1992_03 |
|---|
| ORD ID | ord-356015debd6a47fb9674b9834b98e589 |
|---|
| Source note | uspto-grants-1992_03 |
|---|
