HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2371991Generated: November 3, 2026
2,6-Dimethoxybenzoyl chloride → HCID 14366290, compound
https://huagongshe.com/reaction/2371991
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,6-Dimethoxybenzoyl chloride | HCID 74810 | — |
| Reactant | 6-methoxy-(6H)-dibenz[c,e][1,2]-oxaphosphorin | HCID 11436148 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14366290 | HCID 14366290 | — |
Reaction Steps
60.1 g (0.3 mol) of 2,6-dimethoxybenzoyl chloride were warmed to 85° C. under a nitrogen atmosphere. 69 g (0.3 mol) of 6-methoxy-(6H)-dibenz[c,e][1,2]oxaphosphorin were added dropwise while stirring. The temperature was then slowly increased to 125° C. When the reaction was complete and after cooling, 150 ml of toluene were added. After crystallization, 99 g (87% of theory) of the abovementioned compound of melting point 96° to 98° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05096935 |
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| Source dataset | uspto-grants-1992_03 |
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| ORD ID | ord-5ab2658461fd4abeaf09cc69d36c1b2a |
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| Source note | uspto-grants-1992_03 |
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