Hydrochloric Acid → HCID 21694998, compound

Participants

Reaction Steps

A suspension of platinum oxide (0.3 g), in a solution of XVII (16.71 g, 88 mmol) in ethanol (100 mL) and concentrated HCl (17.6 g, 176 mmol), was hydrogenated in a 500 mL Parr bottle at 60 psi and room temperature for 24 hr. The mixture was then filtered. The filtrate was concentrated in vacuo to give the product as a white powder which was used in the next step without further purification.

Provenance & Evidence